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Please use this identifier to cite or link to this item: https://hdl.handle.net/2440/86637
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dc.contributor.authorBecker, A.M.-
dc.contributor.authorIrvine, R.W.-
dc.contributor.authorMcCormick, A.S.-
dc.contributor.authorRussell, R.A.-
dc.contributor.authorWarrener, R.N.-
dc.date.issued1986-
dc.identifier.citationTetrahedron Letters: the international journal for the rapid publication of all preliminary communications in organic chemistry, 1986; 27(29):3431-3434-
dc.identifier.issn0040-4039-
dc.identifier.issn1873-3581-
dc.identifier.urihttp://hdl.handle.net/2440/86637-
dc.description.abstractLithiation (n-BuLi) of the (3′-methoxyphenyl) oxazoline (2a) occurs specifically at C2′ and, following carboxylation (CO2/13CO2) and esterification, yields the phthalate derivative (e.g.5a). Elaboration of the oxazoline-ring furnishes the related aldehydes which spontaneously cyclise to form the 3-hydroxyphthalides (8/10). The title[5-13C] anthracyclinone (20) is produced from 3-cyanophthalide (11) in good yield and with excellent isotopic efficiency.-
dc.description.statementofresponsibilityAnna M. Becker, Robert W. Irvine, Alison S. McCormick, Richard A. Russell, Ronald N. Warrener-
dc.language.isoen-
dc.publisherPergamon Press-
dc.rightsCopyright status unknown-
dc.source.urihttp://dx.doi.org/10.1016/s0040-4039(00)84815-7-
dc.titleA new route to 3-hydroxyphthalides: application to the synthesis of racemic [5-¹³C] daunomycinone-
dc.title.alternativeA new route to 3-hydroxyphthalides: application to the synthesis of racemic [5-(13)C] daunomycinone-
dc.typeJournal article-
dc.identifier.doi10.1016/S0040-4039(00)84815-7-
pubs.publication-statusPublished-
Appears in Collections:Aurora harvest 2
Chemistry publications

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